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Pulse methods in 1D and 2D liquid-phase NMR
Title:
Pulse methods in 1D and 2D liquid-phase NMR
Author:
Brey, Wallace S.
ISBN:
9781299536111
9780080917030
Publication Information:
San Diego, Calif. : Academic Press, ©1988.
Physical Description:
1 online resource (x, 561 pages) : illustrations
Contents:
Front Cover; Pulse Methods in 1D and 2D Liquid-Phase Nmr; Copyright Page; Table of Contents; Preface; CHAPTER 1. Basic Methods and Simple Pulsed Experiments; I. Introduction; II. Spin-Echo Experiments; III. Polarization-Transfer Experiments; IV. Experimental Aspects of Pulsed NMR; References; CHAPTER 2. Density-Operator Theory of Pulses and Precession; I. Introduction; II. Overview; III. Theory and Use of Product Operators; IV. A Typical Two-Dimensional Experiment-Double-Quantum Spectroscopy of Two Coupled Spins-1/2; V. Summary; Acknowledgments; References
CHAPTER 3. Polarization Transfer and Editing Techniques*I. Introduction; II. Theory; III. Polarization Transfer and Purging; IV. Heteronuclear Spectral Editing Techniques; Appendixes; Acknowledgment; References; CHAPTER 4. Principles of Multiple-Quantum Spectroscopy; I. Introduction; II. Operator Formalism; III. Multiple-Quantum Coherence for a System of Two Spin-1/2 Nuclei; IV. Order-Selective Detection; V. Multiple-Quantum Coherences for Systems Containing Three or More Spin-1/2 Nuclei; VI. Summary; Acknowledgments; References
CHAPTER 5. Applications of Two-Dimensional NMR Experiments in LiquidsI. Introduction; II. Instrumental Requirements; III. J-Resolved 2D NMR; IV. Chemical Shift Correlation 2D NMR; V. Shift Correlation by Relayed Coherence-Transfer 2D NMR; VI. Magnetization-Transfer 2D NMR; VII. Zero- and Multiple-Quantum 2D Methods; References; CHAPTER 6. Applications of 2D NMR to Biological Systems; I. Introduction; II. The Basic 2D NMR Experiments for Spectral Assignment and Structure Elucidation; III. Advanced Methods for Biological Samples; IV. Structural Analysis of Biomolecules; References
CHAPTER 7. Multiple-Resonance and Two-Dimensional NMR Techniques in Analysis of Fluorocarbon Compounds and PolymersI. Introduction; II. Resolution Enhancement and Proton Decoupling; III. Two-Dimensional NMR; IV. Experimental Details; V. Summary; References; CHAPTER 8. Recent Developments in Pulsed NMR Methods; I. RELAY and Observation by Hydrogen Detection; II. Homonuclear Correlation; III. Isotropic Mixing Experiments; IV. Applications of Zero-Quantum Coherence; V. Nuclear Overhauser Enhancement; References; Appendix: Reading List; Index
Abstract:
FROM THE PREFACE: Pulse Methods in 1D and 2D Liquid-Phase NMR is written to enable the practicing NMR spectroscopist to understand and apply the varied and powerful new techniques developed in the past few years for obtaining spectra with greatly increased information content and from smaller and smaller samples. The intent is to describe both theory and practice in simple and detailed fashion so that the methods may be critically evaluated and effectively used in any potential application. As methods become more complex they require more instrument time, and it is important to be able to judge whether the investment of this time is justified. It is also essential for the spectroscopist to be in a position to evaluate the capabilities of the instrumentation available, as well as the additional requirements for utilization of particular new methods. The material in this book assumes a knowledge of continuous-wave NMR methods as well as an elementary understanding of the normal pulsed Fourier-transform spectroscopic procedures, together with a knowledge of such related phenomena as the nuclear Overhauser effect. Although much of the treatment is necessarily methematical, this aspect of the presentation has been simplified as much as possible.
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Pulse methods in one D and two D liquid-phase NMR.
Electronic Access:
ScienceDirect http://www.sciencedirect.com/science/book/9780121331559Available:*
Shelf Number | Item Barcode | Shelf Location | Status |
|---|---|---|---|
| QD96 .N8 P85 1988 | 1177454-1001 | Elsevier E-Book Collections | Searching... |
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