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Organic Synthesis and Characterization of Luminol Derivatives
Başlık:
Organic Synthesis and Characterization of Luminol Derivatives
Yazar:
Whippie, Drew Lee Ann, author.
ISBN:
9780438080850
Yazar Ek Girişi:
Fiziksel Tanımlama:
1 electronic resource (51 pages)
Genel Not:
Source: Masters Abstracts International, Volume: 57-06M(E).
Advisors: Jin Jin Committee members: Andrea Alveshere; Jin Jin; Liguo Song; Shaozhong Zhang.
Özet:
Luminol was first synthesized in 1908. It however was not used for blood testing until it was first described for that use by Walter Sprech in 1937. Since that time, luminol has expanded its usefulness in forensic science but also in many other chemistry fields. Luminol has also been used to synthesize derivatives of luminol. Luminol has a few important drawbacks: heat sensitivity, light sensitivity, and the reaction is short lived. One such derivative was used to evaluate heavy metals in a water sample; the results showed that the derivative had good selectivity and reproducibility. This such derivative can then be used in a real world application to test for heavy metals in water supplies. Our research is to synthesize new luminol derivatives that will have an increased conjugation, stability, and water solubility. The luminol derivatives were synthesized using luminol as one of the starting materials and their chemical structures were characterized by Nuclear Magnetic Resonance Spectroscopy (NMR) and Ultraviolet/Visible Spectroscopy (UV/Vis). All the derivatives were found to have luminescent properties when tested with K3Fe(CN)6. The luminol derivatives synthesized were found to react with horse blood and a common household inference, bleach.
Notlar:
School code: 6012
Konu Başlığı:
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Yer Numarası | Demirbaş Numarası | Shelf Location | Lokasyon / Statüsü / İade Tarihi |
---|---|---|---|
XX(692536.1) | 692536-1001 | Proquest E-Tez Koleksiyonu | Arıyor... |
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